Author: Li, Ling; Long, Jing; Li, Long; Cao, Huijuan; Tang, Tingting; Xi, Xinghua; Qin, Ling; Lai, Yuxiao; Wang, Xinluan
Title: Quantitative determination of residual 1,4-dioxane in three-dimensional printed bone scaffold Document date: 2017_7_17
ID: qd2te842_32
Snippet: Robustness of the method Robustness can be described as the ability to reproduce the (analytical) method under different circumstances. When a small change exists, a robust test is set up to evaluate the robustness of a method. Special factors changed in GC-MS detection were columns of different brands or batch numbers, different solid phase, different types of supports, flow rate of carrier gas, temperature of column, inlet, and detection [26] ......
Document: Robustness of the method Robustness can be described as the ability to reproduce the (analytical) method under different circumstances. When a small change exists, a robust test is set up to evaluate the robustness of a method. Special factors changed in GC-MS detection were columns of different brands or batch numbers, different solid phase, different types of supports, flow rate of carrier gas, temperature of column, inlet, and detection [26] . In this validation, we used two different columns (HP-5ms and DB-624) to detect the same sample for evaluating the robustness. Each column detected samples in triplicate.
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