Author: Becker, Daniel; Kaczmarska, Zuzanna; Arkona, Christoph; Schulz, Robert; Tauber, Carolin; Wolber, Gerhard; Hilgenfeld, Rolf; Coll, Miquel; Rademann, Jörg
Title: Irreversible inhibitors of the 3C protease of Coxsackie virus through templated assembly of protein-binding fragments Document date: 2016_9_28
ID: 0oq4kkn5_19
Snippet: After addition of 2 (100 mg, 0. 5 mmol, 0.1 eq) sodium cyanoborohydride (62 mg, 1 mmol, 2 eq) was added and the solution was stirred for twelve hours. The reaction was quenched with water, the solvent removed in vacuo and the residue was purified with reversed phase high performance liquid chromatography, yielding 7 as a white solid......
Document: After addition of 2 (100 mg, 0. 5 mmol, 0.1 eq) sodium cyanoborohydride (62 mg, 1 mmol, 2 eq) was added and the solution was stirred for twelve hours. The reaction was quenched with water, the solvent removed in vacuo and the residue was purified with reversed phase high performance liquid chromatography, yielding 7 as a white solid.
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