Author: Pahon?u, Elena; Ilie?, Diana-Carolina; Shova, Sergiu; Paraschivescu, Codru?a; Badea, Mihaela; Gulea, Aurelian; Ro?u, Tudor
Title: Synthesis, Characterization, Crystal Structure and Antimicrobial Activity of Copper(II) Complexes with the Schiff Base Derived from 2-Hydroxy-4-Methoxybenzaldehyde Document date: 2015_4_2
ID: 0wcvoygd_33
Snippet: A solution of 2-hydroxy-4-methoxybenzaldehyde (0.152 g, 1 mmoL) in ethanol (10 mL) was added to a solution of ethyl-4-aminobenzoate (0.165 g, 1 mmoL) in ethanol (20 mL). The mixture was stirred for 1 h at 25 °C, then refluxed for 4 h and kept at 4 °C for several days. The characteristic yellow precipitate obtained by Schiff base condensation was filtered out and kept for crystallization. Fine yellow crystals obtained upon slow evaporation at ro.....
Document: A solution of 2-hydroxy-4-methoxybenzaldehyde (0.152 g, 1 mmoL) in ethanol (10 mL) was added to a solution of ethyl-4-aminobenzoate (0.165 g, 1 mmoL) in ethanol (20 mL). The mixture was stirred for 1 h at 25 °C, then refluxed for 4 h and kept at 4 °C for several days. The characteristic yellow precipitate obtained by Schiff base condensation was filtered out and kept for crystallization. Fine yellow crystals obtained upon slow evaporation at room temperature were characterized, including single crystal X-ray diffraction.
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