Author: Tursynbolat, Satar; Bakytkarim, Yrysgul; Huang, Jianzhi; Wang, Lishi
Title: Highly sensitive simultaneous electrochemical determination of myricetin and rutin via solid phase extraction on a ternary Pt@r-GO@MWCNTs nanocomposite Document date: 2019_3_22
ID: 00n9xho8_8
Snippet: A novel one-pot method was used to synthesize the ternary Pt@r-GO@MWCNTs nanocomposites at room conditions (room temperature is 25 C) (Scheme 1). First, 30 mg of monolayer graphene oxide and 30 mg of MWCNTs were placed in 30 mL of double distilled water and mixed for 30 min under ultrasonication. Subsequently, under stirring conditions, 500 mL of a 60 mM H 2 PtCl 6 solution was added to the above solution. Simultaneously, 10 mL of a 0.05 g/mL NaB.....
Document: A novel one-pot method was used to synthesize the ternary Pt@r-GO@MWCNTs nanocomposites at room conditions (room temperature is 25 C) (Scheme 1). First, 30 mg of monolayer graphene oxide and 30 mg of MWCNTs were placed in 30 mL of double distilled water and mixed for 30 min under ultrasonication. Subsequently, under stirring conditions, 500 mL of a 60 mM H 2 PtCl 6 solution was added to the above solution. Simultaneously, 10 mL of a 0.05 g/mL NaBH 4 solution was added and the reaction mixture was stirred vigorously for 30 min. The product was washed three times with a mixed solution of ethanol and water at a ratio of 1:1. Finally, 8 mL of an ethanol and water mixture at a ratio of 1:3 was added to the product, yielding the ternary Pt@r-GO@MWCNTs nanocomposite.
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